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Sodium Cyanide → 2-(2,6-Dimethylpiperidino)amino-3-phenoxypropionitrile
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Sodium Cyanide | HCID 8929 | — |
| 反応物 | Phenoxyacetaldehyde | HCID 75033 | — |
| 反応物 | 2,6-Dimethyl-1-piperidylamine | HCID 123482 | — |
| 生成物 | 2-(2,6-Dimethylpiperidino)amino-3-phenoxypropionitrile | HCID 19915654 | 76.2% |
反応手順
12.8 g of 1-amino-2,6-dimethylpiperidine, 5.4 g of sodium cyanide and 15.0 g of phenoxyacetaldehyde are reacted analogously to 8a). 20.8 g of 2-(2,6-dimethylpiperidino)amino-3-phenoxypropionitrile are obtained, which are employed in the following step without further purification
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05079244 |
| 出典データセット | uspto-grants-1992_01 |
| ORD ID | ord-6488102a1b7b4334bf2b2615994185af |
| 出典メモ | uspto-grants-1992_01 |