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Sodium Cyanide → 3-Benzyloxy-2-((2,6-dimethylpiperidino)amino)propionitrile
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Sodium Cyanide | HCID 8929 | — |
| 反応物 | (Phenylmethoxy)acetaldehyde | HCID 108989 | — |
| 反応物 | 2,6-Dimethyl-1-piperidylamine | HCID 123482 | — |
| 生成物 | 3-Benzyloxy-2-((2,6-dimethylpiperidino)amino)propionitrile | HCID 19915656 | 81.2% |
反応手順
12.8 g of 1-amino-2,6-dimethylpiperidine, 4.9 g of sodium cyanide and 15.0 g of benzyloxyacetaldehyde are reacted analogously to 8a). 23.3 g of 3-benzyloxy-2-((2,6-dimethylpiperidino)amino)propionitrile are obtained, which are employed in the following step without further purification.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05079244 |
| 出典データセット | uspto-grants-1992_01 |
| ORD ID | ord-047c45d38cb140d885c8626a3ed8984d |
| 出典メモ | uspto-grants-1992_01 |