5,6,7,8-Tetrahydro-2-naphthol → HCID 19914429、化合物
反応式
[OH-].[K+].[CH:3]1[C:12]2[CH2:11][CH2:10][CH2:9][CH2:8][C:7]=2[CH:6]=[CH:5][C:4]=1[OH:13].[CH3:14][C:15]1[CH:16]=[C:17]([CH:22]=[CH:23][CH:24]=1)[O:18][CH2:19][CH2:20]Cl>O>[CH3:14][C:15]1[CH:16]=[C:17]([CH:22]=[CH:23][CH:24]=1)[O:18][CH2:19][CH2:20][O:13][C:4]1[CH:5]=[CH:6][C:7]2[CH2:8][CH2:9][CH2:10][CH2:11][C:12]=2[CH:3]=1参加物
5
実験手順
4.0 g (0.06 mol) of 85% potassium hydroxide was dissolved in 25 g of distilled water and 7.4 g (0.05 mol) of 5,6,7,8-tetrahydro-β-naphthol was dissolved in the formed solution. 8.5 g (0.05 mol) of 2-(3-methylphenoxy)ethyl chloride was added to the solution and the mixture was stirred under reflux for 3 h.
後処理
- temperatureunder reflux for 3 h.
出典と根拠
- ORDレコード
- ord-38a6530c73614189909be25893fbc6ec
- 出典データセット
- uspto-grants-1992_01
- 特許番号
- US05081099
反応ノート
読み込み中…