Oxalic Acid → Carbonate oxalate

HRID 1092781

反応式

HRID 1092781 の反応式
[C:1](=[O:4])([O-:3])[O-:2].[C:5]([OH:10])(=[O:9])[C:6]([OH:8])=[O:7]>C(OCC)(=O)C>[C:5]([OH:10])(=[O:9])[C:6]([OH:8])=[O:7].[C:1](=[O:2])([OH:4])[OH:3]

参加物

4

反応物 2

HCID 971Oxalic AcidHCID 19660Carbonate Ion

生成物 1

HCID 88099579Carbonate oxalate

試薬・触媒・溶媒 1

HCID 8857Ethyl Acetate溶媒2 回

実験手順

In 7 mL of ethyl acetate was dissolved 0.31 g of 1-{3-[2-(1-benzothiophen-5-yl)ethoxy]propyl}-3-azetidinyl=methyl=carbonate, and to the solution was added a solution of 0.10 g of oxalic acid in 1 mL of ethyl acetate, after which the resulting mixture was stirred at room temperature. The crystals precipitated were collected by filtration to obtain 0.34 g of 1-{3-[2-(1-benzothiophen-5-yl)ethoxy]propyl}-3-azetidinyl=methyl=carbonate oxalate.

後処理

  1. customThe crystals precipitated
  2. filtrationwere collected by filtration

出典と根拠

ORDレコード
ord-3b8027318e3b489a96a87e47a57ab7e9
出典データセット
uspto-grants-2012_03
特許番号
US08129535B2

関連ノート

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