化工社化工社 化学情報印刷レポート · 研究参考用
4-Nitroisophthalic acid → 4-Aminobenzene-1,3-dioic acid
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 4-Nitroisophthalic acid | HCID 3062438 | — |
| 触媒 | Palladium | HCID 23938 | — |
| 溶媒 | Methanol | HCID 887 | — |
| 生成物 | 4-Aminobenzene-1,3-dioic acid | HCID 11355852 | — |
反応手順
To a solution of 4-nitro isophthalic acid (4 g, 18.95 mmol) in MeOH (200 mL) was added Pd/C (20%) and the mixture was hydrogenated at RT over night. The reaction mixture was filtered through Celite and filtrate concentrated under vacuum to give 4-amino isophthalic acid in 60% as a solid.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08133998B2 |
| 出典データセット | uspto-grants-2012_03 |
| ORD ID | ord-a70aad4b64f84b4ba0494f54b48628cb |
| 出典メモ | uspto-grants-2012_03 |