2-Acrylamido-2-methyl-1-propanesulfonic acid → Ammonium acryloyldimethyltaurate

HRID 1094915

反応式

HRID 1094915 の反応式
COCCOCC[N:8](CCOCCOC)CCOCCOC.[C:23]([NH:27][C:28]([CH3:35])([CH3:34])[CH2:29][S:30]([OH:33])(=[O:32])=[O:31])(=[O:26])[CH:24]=[CH2:25]>>[NH4+:8].[C:23]([NH:27][C:28]([CH3:35])([CH3:34])[CH2:29][S:30]([O-:33])(=[O:31])=[O:32])(=[O:26])[CH:24]=[CH2:25]

参加物

3

反応物 2

HCID 653602-Acrylamido-2-methyl-1-propanesulfonic acidHCID 112414Ethanamine, 2-(2-methoxyethoxy)-N,N-bis[2-(2-methoxyethoxy)ethyl]-

生成物 1

HCID 6850854Ammonium acryloyldimethyltaurate収率 99%

実験手順

A nitrogen purged 50 ml schlenk flask was charged with freshly distilled tris[2-(2-methoxyethoxy)-ethyl]amine (1.69 g, 5.24 mmol) and 2-acrylamido-2-methyl-1-propanesulfonic acid (1.09 g, 5.24 mmol) and stirred at ambient temperature for 8 hr or until completely dissolved. Total dissolution completes formation of the AMPS ammonium salt monomer as a transparent light amber oil in a 99% yield which was used immediately without further purification.

後処理

  1. customA nitrogen purged 50 ml schlenk flask
  2. dissolutionuntil completely dissolved
  3. dissolutionTotal dissolution
  4. customwas used immediately without further purification

出典と根拠

ORDレコード
ord-f3d5db68fd8a4c70a4ffb95307229953
出典データセット
uspto-grants-2012_03
特許番号
US08134024B2

関連ノート

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