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3-Chloro-2,6-difluorophenol → 7-{2-[2-(3-Chloro-2,6-difluorophenoxy)ethoxy]thiazol-5-yl}-6-[cyclopropyl-(3-methoxy-2-methylbenzyl)carbamoyl]-3,9-diazabicyclo[3.3.1]non-6-ene-3,9-dicarboxylic acid di-tert-butyl ester
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 3-Chloro-2,6-difluorophenol | HCID 2773564 | — |
| 反応物 | 6-[Cyclopropyl-(3-methoxy-2-methylbenzyl)carbamoyl]-7-[2-(2-hydroxyethoxy)thiazol-5-yl]-3,9-diazabicyclo[3.3.1]non-6-ene-3,9-dicarboxylic acid di-tert-butyl ester | HCID 68570797 | — |
| 生成物 | 7-{2-[2-(3-Chloro-2,6-difluorophenoxy)ethoxy]thiazol-5-yl}-6-[cyclopropyl-(3-methoxy-2-methylbenzyl)carbamoyl]-3,9-diazabicyclo[3.3.1]non-6-ene-3,9-dicarboxylic acid di-tert-butyl ester | HCID 69085301 | — |
反応手順
This compound is prepared from compound E9 and 3-chloro-2,6-difluorophenol, according to the above-described procedure A. LC-MS: tR=1.23 min, ES+: 831.38.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08138340B2 |
| 出典データセット | uspto-grants-2012_03 |
| ORD ID | ord-bfe9995b0c3746f5b3545fdc64dafde7 |
| 出典メモ | uspto-grants-2012_03 |