4,6-Dinitrobenzene-1,3-diamine → 1,2,4,5-Benzenetetraamine

HRID 1099502

反応式

HRID 1099502 の反応式
[H][H].[NH2:3][C:4]1[C:9]([N+:10]([O-])=O)=[CH:8][C:7]([N+:13]([O-])=O)=[C:6]([NH2:16])[CH:5]=1>>[NH2:3][C:4]1[CH:5]=[C:6]([NH2:16])[C:7]([NH2:13])=[CH:8][C:9]=1[NH2:10]

参加物

3

実験手順

contacting the reaction mixture formed in step (f) with hydrogen at a pressure in the range of about 0.31 to about 3.45 MPa and a temperature in the range of about 20° C. to about 100° C. to hydrogenate the 1,3-diamino-4,6-dinitrobenzene and produce 1,2,4,5-tetraminobenzene;

後処理

  1. customin the range of about 20° C. to about 100° C.

出典と根拠

ORDレコード
ord-6d0b0fb4d4944ee8b6126071f21b8cd8
出典データセット
uspto-grants-2012_03
特許番号
US08143450B1

関連ノート

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