関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Butyl(dimethyl)silane | HCID 2757279 | — |
| 反応物 | Oxirane, [(10-undecenyloxy)methyl]- | HCID 10353667 | — |
| 生成物 | 11-(Butyldimethylsilyl)undecyl glycidyl ether | HCID 19694625 | 82.6% |
反応手順
A 100-ml flask equipped with a stirrer was charged with 13.6 g (60 mmol) of 10-undecenyl glycidyl ether, 5.8 g (50 mmol) of butyldimethylsilane and 4 mg (0.01 mmol) of H2PtCl6. The contents were stirred at 60° C. for 24 hours. The resultant reaction mixture was distilled under reduced pressure (145°-154° C./6×10-3 Torr), thereby obtaining 14.15 g (yield: 82.6%) of 11-(butyldimethylsilyl)undecyl glycidyl ether.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US05723497 |
|---|
| 出典データセット | uspto-grants-1998_03 |
|---|
| ORD ID | ord-3d817c6e53494262853c2c135e11aa2f |
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| 出典メモ | uspto-grants-1998_03 |
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