Octylamine → N-Heptyl-N'-octylthiourea

HRID 1105828

反応式

HRID 1105828 の反応式
[CH2:1]([N:8]=[C:9]=[S:10])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH3:7].[CH2:11]([NH2:19])[CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH3:18]>C1C=CC=CC=1>[CH2:1]([NH:8][C:9]([NH:19][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH3:18])=[S:10])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH3:7]

参加物

4

反応物 2

HCID 8143OctylamineHCID 78152Heptane, 1-isothiocyanato-

生成物 1

HCID 12796254N-Heptyl-N'-octylthiourea収率 105.2%

試薬・触媒・溶媒 1

HCID 241Benzene溶媒

実験手順

To a solution of 3.14 grams (0.02 mole) n-heptylisothiocyanate dissolved in 15 milliliters of benzene is added 2.58 grams (0.02 mole) n-octylamine. The temperature rose to 41° C. The mixture was then refluxed on a steam-bath for about 20 minutes, until the mixture reached a neutral pH. The solution was then evaporated under vacuum. A yield of 6.03 grams of 1-n-heptyl-3-n-octylthiourea was obtained.

後処理

  1. customrose to 41° C
  2. temperatureThe mixture was then refluxed on a steam-bath for about 20 minutes, until the mixture
  3. customThe solution was then evaporated under vacuum

出典と根拠

ORDレコード
ord-f2ffe0eb4f944759889d5de5e67aff59
出典データセット
uspto-grants-1982_01
特許番号
US04310539

関連ノート

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