化工社化工社 化学情報印刷レポート · 研究参考用
Amyl Acetate → Amyl 3-Hydroxy-3-methyl-3-(4-pyridyl)propionate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Amyl Acetate | HCID 12348 | — |
| 反応物 | 4-Acetylpyridine | HCID 14282 | — |
| 生成物 | Amyl 3-Hydroxy-3-methyl-3-(4-pyridyl)propionate | HCID 20441861 | — |
反応手順
A 100 milligram quantity of the hydroxy ester described in Example III is pyrolyzed in a sealed tube at 400° C. for 3 minutes. Analysis of the pyrolysis mixture by gas chromatography indicates the presence of about 30% of a mixture in a 1:1 ratio of amyl acetate and 4-acetylpyridine. The remainder of the mixture contains unreacted starting material.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04312368 |
| 出典データセット | uspto-grants-1982_01 |
| ORD ID | ord-f9b23d518ce24be28e1dde3284ee6ee2 |
| 出典メモ | uspto-grants-1982_01 |