化工社化工社 化学情報印刷レポート · 研究参考用
Cyanamide → HCID 178483888、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Cyanamide | HCID 9864 | — |
| 反応物 | 4-[2-(Dimethylamino)ethoxy]aniline | HCID 6484655 | — |
| 反応物 | HCID 178419082 | HCID 178419082 | — |
| 溶媒 | Nitric Acid | HCID 944 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | HCID 178483888 | HCID 178483888 | — |
反応手順
4-(2-Dimethylaminoethoxy)phenylguanidinium dinitrate was prepared by the method described for 3,4,5-trimethoxyphenylguanidinium nitrate in Example 1 from 4-(2-dimethylaminoethoxy)aniline (5.0 g, 28 mmol), cyanamide (1.75 g, 41 mmol) in water (3.5 ml) and concentrated nitric acid (4 ml) to give the product as a light purple solid (6.8 g) m.p. 149-152°. MS (ES+) 223 (MH+, 100%).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06057329 |
| 出典データセット | uspto-grants-2000_05 |
| ORD ID | ord-542a175815584c18b38a775450c59ee7 |
| 出典メモ | uspto-grants-2000_05 |