化工社化工社 化学情報印刷レポート · 研究参考用
4-(Difluoromethoxy)benzyl alcohol → 1-(2-Butenyl)-7-(4-difluoromethoxybenzyloxy)-2,3-dimethylpyrrolo[2,3-d]pyridazine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 4-(Difluoromethoxy)benzyl alcohol | HCID 2736996 | — |
| 反応物 | 1-(2-Butenyl)-7-chloro-2,3-dimethylpyrrolo[2,3-d]pyridazine | HCID 53719624 | — |
| 生成物 | 1-(2-Butenyl)-7-(4-difluoromethoxybenzyloxy)-2,3-dimethylpyrrolo[2,3-d]pyridazine | HCID 53682881 | 37.8% |
反応手順
The title compound (cis/trans=21/79) was prepared as a white powder in 37.8% yield in a similar procedure to that described in Example 1 by using 1-(2-butenyl)-7-chloro-2,3-dimethylpyrrolo[2,3-d]pyridazine (cis/trans=20/80) and 4-difluoromethoxybenzyl alcohol.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06063782 |
| 出典データセット | uspto-grants-2000_05 |
| ORD ID | ord-55dac3f409764200bde777084ec3c99f |
| 出典メモ | uspto-grants-2000_05 |