化工社化工社 化学情報印刷レポート · 研究参考用
2-Chloro-6-fluorobenzyl alcohol → 1-(2-Butenyl)-7-(2-chloro-6-fluorobenzyloxy)-2,3-dimethylpyrrolo[2,3-d]pyridazine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-Chloro-6-fluorobenzyl alcohol | HCID 91868 | — |
| 反応物 | 1-(2-Butenyl)-7-chloro-2,3-dimethylpyrrolo[2,3-d]pyridazine | HCID 53719624 | — |
| 生成物 | 1-(2-Butenyl)-7-(2-chloro-6-fluorobenzyloxy)-2,3-dimethylpyrrolo[2,3-d]pyridazine | HCID 53716849 | 57.6% |
反応手順
The title compound (cis/trans=21/79) was prepared as a pale brown powder in 57.60% yield in a similar procedure to that described in Example 1 by using 1-(2-butenyl)-7-chloro-2,3-dimethylpyrrolo[2,3-d]pyridazine (cis/trans=24/76) and 2-chloro-6-fluorobenzyl alcohol.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06063782 |
| 出典データセット | uspto-grants-2000_05 |
| ORD ID | ord-b399ab50b4964b8d832710991b0613ed |
| 出典メモ | uspto-grants-2000_05 |