関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | H acid | HCID 7009 | — |
| 反応物 | Cyanuric chloride | HCID 7954 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | 1-Hydroxy-8-(2,4-dichloro-s-triazin-6-ylamino-)naphthalene-3,6-disulphonic acid | HCID 11048924 | — |
反応手順
An ice cold neutral solution of 1-hydroxy-8-aminonaphthalene-3,6-disulphonic acid (31.9 parts) in water (120 parts) was added, with stirring, to a freshly prepared suspension of 2,4,6-trichloro-s-triazine (18.5 parts) in ice and water (140 parts). The mixture was stirred for 3 hours at 0 to 5° C. to give a solution of 1-hydroxy-8-(2,4-dichloro-s-triazin-6-ylamino-)naphthalene-3,6-disulphonic acid (solution 1).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US06068667 |
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| 出典データセット | uspto-grants-2000_05 |
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| ORD ID | ord-96c6ea8add314387a32fb0ab620e9b4d |
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| 出典メモ | uspto-grants-2000_05 |
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