関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | 2-(Methylamino)ethanol | HCID 8016 | — |
| 反応物 | 1,2-Epoxyoctadecane | HCID 23872 | — |
| 溶媒 | Ethanol | HCID 702 | — |
| 生成物 | N-2-Hydroxyethyl-N-2-hydroxyoctadecyl-N-methyl amine | HCID 19694636 | 67% |
反応手順
A 300-ml flask equipped with a stirrer was charged with 26.85 g (0.1 mol) of 1,2-epoxyoctadecane, 7.51 g (0.1 mol) of N-methylethanolamine and 50 ml of ethanol, and the contents were stirred at 80° C. for 18 hours. After the solvent was distilled off under reduced pressure, the resultant residue was purified by column chromatography on silica gel, thereby obtaining 23.0 g (yield: 67%) of the title compound (IIc-2).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US05723497 |
|---|
| 出典データセット | uspto-grants-1998_03 |
|---|
| ORD ID | ord-b816d25167cf4c2ca0b10e123324d743 |
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| 出典メモ | uspto-grants-1998_03 |
|---|
