化工社化工社 化学情報印刷レポート · 研究参考用
2-Octanol → Propan-2-yl 2-dodecylbenzene-1-sulfonate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-Octanol | HCID 20083 | — |
| 反応物 | p-Toluenesulfonic acid 1-methylheptyl ester | HCID 3912199 | — |
| 反応物 | 2-Dodecylbenzene-1-sulfonyl chloride | HCID 20439001 | — |
| 生成物 | Propan-2-yl 2-dodecylbenzene-1-sulfonate | HCID 23368822 | 83% |
反応手順
In the Example of preparation of material 18, 2-octanol was used in place of 2-propanol in the Example of preparation of material 17. In the Example of preparation of material 19, dodecylbenzene sulfonyl chloride was used in place of p-toluene sulfonyl chloride in the Example of preparation of material 17. Other procedures were made in the same way as the Example of preparation of material 17. In the Example of preparation of material 18, 1-methylheptyl p-toluene sulfonate was obtained in the yield of 72% and, in the Example of preparation of material 19, 1-methylethyl dodecylbenzene sulfonate was obtained in the yield of 83%.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05319024 |
| 出典データセット | uspto-grants-1994_06 |
| ORD ID | ord-fcde6d5423e74d30ae06c643be62027b |
| 出典メモ | uspto-grants-1994_06 |