関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Carbon Dioxide | HCID 280 | — |
| 反応物 | Water | HCID 962 | — |
| 反応物 | 2,6-Dichlorophenoxysulfonyl isocyanate | HCID 19018468 | — |
| 溶媒 | Carbon Tetrachloride | HCID 5943 | — |
| 生成物 | 2,6-Dichlorophenyl sulfamate | HCID 19018467 | — |
反応手順
2.6 ml of water are added dropwise at 30° C. to 40° C. to a solution of 24.4 g of 2,6-dichlorophenoxysulfonyl isocyanate in 200 ml of tetrachloromethane. The mixture is then stirred at room temperature until the evolution of carbon dioxide is complete and cooled to 0° C., the product is filtered off with suction and the residue is then washed with ice-cold tetrachloromethane. After drying in vacuo, 21.4 g of 2,6-dichlorophenyl sulfamate of melting point 108°-110° C. are obtained.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US05324710 |
|---|
| 出典データセット | uspto-grants-1994_06 |
|---|
| ORD ID | ord-e54d7659cfb745089cd80515edce33e1 |
|---|
| 出典メモ | uspto-grants-1994_06 |
|---|
