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Benzyltriphenylphosphonium bromide → 6-Methoxy-2-[2-phenylethenyl]-1H-indole
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Benzyltriphenylphosphonium bromide | HCID 2734970 | — |
| 反応物 | 6-Methoxy-1H-indole-2-carbaldehyde | HCID 21980688 | — |
| 生成物 | 6-Methoxy-2-[2-phenylethenyl]-1H-indole | HCID 73123140 | 94% |
反応手順
Reaction of 6-methoxyindole-2-carboxaldehyde (145) with benzyltriphenylphosphonium bromide using the procedure described in example 37 gave (146) (94%) as a white solid (mixture of E/Z isomers) which was used without further purification.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07094798B1 |
| 出典データセット | uspto-grants-2006_08 |
| ORD ID | ord-44e17ed999e24f12a40be8ec409048b0 |
| 出典メモ | uspto-grants-2006_08 |