関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | 2,4-Dihydroxybenzophenone | HCID 8572 | — |
| 反応物 | Glycidoxypropyltrimethoxysilane | HCID 17317 | — |
| 触媒 | Tetramethylammonium chloride | HCID 6379 | — |
| 生成物 | 2,4-DIHYDROXYBENZOPHENONE gamma-GLYCIDOXYPROPYLTRIMETHOXYSILANE | HCID 86736099 | — |
反応手順
The above compound (Adduct I, was prepared by heating a mixture of 10.7 g (0.05 mole) of 2,4-dihydroxybenzophenone and 12.04 g (0.051 mole) of γ-glycidoxypropyltrimethoxysilane under nitrogen in the presence of 0.1 g of tetramethylammonium chloride. The mixture was stirred and gradually heated to 75°-80° C., then maintained at this temperature for 8 hours. During this period it changed into a homogeneous, viscous oil. An equivalent product was obtained when the reactants were heated at 80° C. for 4 hrs.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US04122233 |
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| 出典データセット | uspto-grants-1978_10 |
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| ORD ID | ord-f4c11301f5874c448f4f5995118a4d18 |
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| 出典メモ | uspto-grants-1978_10 |
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