関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Hydrazinecarboxaldehyde | HCID 12229 | — |
| 反応物 | Ethyl thiooxamate | HCID 2733398 | — |
| 生成物 | (N-Formylhydrazino)-imino acetic acid ethyl ester | HCID 86590617 | 76.3% |
反応手順
A mixture of ethyl thioxamate (10.55 g, 79.2 mmol) and formylhydrazine (5.00 g, 83.2 mmol) was heated at 65° C. for 30 minutes and stirred in accordance with a method described in Collect. Czech Chem. Commun., 1984, 49, p 2492. After cooling, the precipitated crystal was collected by filteration and washed with ethanol to give (N-formylhydrazino)-imino acetic acid ethyl ester (9.62 g). Yield: 76%.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US07098201B2 |
|---|
| 出典データセット | uspto-grants-2006_08 |
|---|
| ORD ID | ord-a62cf4c9ffc84cf08a93f17d6e865c73 |
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| 出典メモ | uspto-grants-2006_08 |
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