化工社化工社 化学情報印刷レポート · 研究参考用
Benzyl Bromide → 7-(1-Adamantyl)-6-benzyloxy-2-bromonaphthalene
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Benzyl Bromide | HCID 7498 | — |
| 反応物 | 3-(Adamantan-1-yl)-6-bromonaphthalen-2-ol | HCID 14549072 | — |
| 生成物 | 7-(1-Adamantyl)-6-benzyloxy-2-bromonaphthalene | HCID 22000359 | 80% |
反応手順
Following the basic procedure of Example 11, by reacting 12.5 g (35 mmol) of 7-(1-adamantyl)-6-hydroxy-2-bromonaphthalene with 5 ml (42 mmol) of benzyl bromide, 12.5 g (80%) of the expected compound of melting point 150°-151° C. were obtained.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05723499 |
| 出典データセット | uspto-grants-1998_03 |
| ORD ID | ord-b7fc3759f58e4209a7cf0781050443b3 |
| 出典メモ | uspto-grants-1998_03 |