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1-Iodopropane → methyl N-propyl-4-iodo-2-pyrrolecarboxylate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1-Iodopropane | HCID 33643 | — |
| 反応物 | methyl 4-iodo-1H-pyrrole-2-carboxylate | HCID 11673249 | — |
| 生成物 | methyl N-propyl-4-iodo-2-pyrrolecarboxylate | HCID 19694682 | 64.7% |
反応手順
Following the basic procedure of Example 7(d), by reacting 1.96 g (7.8 mmol) of methyl 4-iodo-2-pyrrolecarboxylate with 940 μl (9.6 mmol) of 3-iodopropane, 1.48 g (64%) of methyl N-propyl-4-iodo-2-pyrrolecarboxylate was obtained in the form of a slightly yellow oil.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05723499 |
| 出典データセット | uspto-grants-1998_03 |
| ORD ID | ord-5fa351dbe3ea452bbf01e7f31dec9368 |
| 出典メモ | uspto-grants-1998_03 |