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4-Fluorobenzyl bromide → 7-(1-Adamantyl)-6-(4-fluorobenzyl)oxy-2-bromonaphthalene
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 4-Fluorobenzyl bromide | HCID 68021 | — |
| 反応物 | 3-(Adamantan-1-yl)-6-bromonaphthalen-2-ol | HCID 14549072 | — |
| 生成物 | 7-(1-Adamantyl)-6-(4-fluorobenzyl)oxy-2-bromonaphthalene | HCID 22000379 | 86% |
反応手順
Following the basic procedure of Example 11, by reacting 1.1 g (3 mmol) of 7-(1-adamantyl)-6-hydroxy-2-bromonaphthalene with 420 μl (3,3 mmol) of 4-fluorobenzyl bromide, 1.2 g (86%) of the expected compound was obtained in the form of a colorless oil.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05723499 |
| 出典データセット | uspto-grants-1998_03 |
| ORD ID | ord-f03bd0e627354ee4a55f5536f5f04cf4 |
| 出典メモ | uspto-grants-1998_03 |