化工社化工社 化学情報印刷レポート · 研究参考用
Boronic Acid → 7-(1-Adamantyl)-6-tert-butyldimethylsilyloxy-2-naphthylboronic acid
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Boronic Acid | HCID 61668 | — |
| 反応物 | 7-(1-Adamantyl)-6-tert-butyldimethylsilyloxy-2-bromonaphthalene | HCID 19694681 | — |
| 生成物 | 7-(1-Adamantyl)-6-tert-butyldimethylsilyloxy-2-naphthylboronic acid | HCID 19694665 | — |
反応手順
Following the basic procedure of Example 7(e), beginning with 11.9 g (25.4 mmol) of 7-(1-adamantyl)-6-tert-butyldimethylsilyloxy-2-bromonaphthalene, 8.37 g (75%) of the expected boronic acid of melting point 221°-222° C. were obtained.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05723499 |
| 出典データセット | uspto-grants-1998_03 |
| ORD ID | ord-3150c5b19251400f94abae6bc2510c0b |
| 出典メモ | uspto-grants-1998_03 |