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Benzenamine, 4-(4-morpholinyl)- → HCID 178418945、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Benzenamine, 4-(4-morpholinyl)- | HCID 75655 | — |
| 反応物 | HCID 178418992 | HCID 178418992 | — |
| 溶媒 | Tetrahydrofuran | HCID 8028 | — |
| 生成物 | HCID 178418945 | HCID 178418945 | — |
反応手順
The named compound is prepared by refluxing 0.020 gms E & Z 3-hydroxymethylene-6-(3-methoxy-phenyl)-1,3-dihydro-indol-2-one with 0.020 gms. 4-morpholin-4-yl-phenylamine in tetrahydrofuran (0.33 mL) for 2 days. Following cooling to room temperature, solvent evaporation in vacuo, trituration with isopropanol and filtration the reaction yields the named compound as a solid in the amount of 15.7 mg.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07098236B2 |
| 出典データセット | uspto-grants-2006_08 |
| ORD ID | ord-e83cfed6237146ecaad1c4492e25a9ff |
| 出典メモ | uspto-grants-2006_08 |