Hydrochloric Acid → HCID 178479216、化合物

HRID 1154119ノート

反応式

HRID 1154119 の反応式
C([NH:4][CH2:5][CH2:6][CH2:7][N:8]1[C:12]([SH:13])=[N:11][N:10]=[N:9]1)(=O)C.[ClH:14]>>[ClH:14].[NH2:4][CH2:5][CH2:6][CH2:7][N:8]1[C:12]([SH:13])=[N:11][N:10]=[N:9]1

参加物

3

反応物 2

HCID 313Hydrochloric AcidHCID 178474793HCID 178474793、化合物

生成物 1

HCID 178479216HCID 178479216、化合物

実験手順

A mixture of 1-(3-acetamidopropyl)-1H-tetrazole-5-thiol (85 g) and 6N hydrochloric acid (1 l) was refluxed for 75 minutes under stirring. The reaction mixture was concentrated in vacuo and precipitates were collected by filtration and washed with hexane and diethyl ether to give 1-(3-aminopropyl)-1H-tetrazole-5-thiol hydrochloride (67.15 g).

後処理

  1. temperaturewas refluxed for 75 minutes
  2. concentrationThe reaction mixture was concentrated in vacuo
  3. customprecipitates
  4. filtrationwere collected by filtration
  5. washwashed with hexane and diethyl ether

出典と根拠

ORDレコード
ord-e626872f8af34a81917dbcb23313e739
出典データセット
uspto-grants-1984_12
特許番号
US04487767

反応ノート

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