化工社化工社 化学情報印刷レポート · 研究参考用
Sulfuric Acid → Octyl 3-mercaptopropionate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Sulfuric Acid | HCID 1118 | — |
| 反応物 | Methyl Acrylate | HCID 7294 | — |
| 反応物 | Octyl acrylate | HCID 17258 | — |
| 生成物 | Octyl 3-mercaptopropionate | HCID 89128 | 80% |
反応手順
The procedure was as described in Example 1 but in place of methyl acrylate there were employed 184 grams of octyl acrylate and first there were added 250 ml of dilute H2SO4 (4N) and the later 300 ml of dilute H2SO4. After the fractional distillation there were isolated 174.5 grams (corresponding to a yield of 80%) of 3-mercaptopropionic acid octyl ester.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04490307 |
| 出典データセット | uspto-grants-1984_12 |
| ORD ID | ord-40168e2812b449e38aa362c27a0deb73 |
| 出典メモ | uspto-grants-1984_12 |