反応式
[OH2:1].[CH2:2]([O:9][C:10]1[CH:15]=[CH:14][CH:13]=[CH:12][C:11]=1[C:16]([CH:18]=O)=O)[C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][CH:4]=1.[CH3:20][CH:21]([NH2:31])[CH2:22][C:23]1[CH:28]=[CH:27][C:26]([O:29][CH3:30])=[CH:25][CH:24]=1>CS(C)=O>[CH3:20][CH:21]([N:31]=[C:10]([O:9][CH2:2][C:3]1[CH:4]=[CH:5][CH:6]=[CH:7][CH:8]=1)[C:15]([C:14]1[CH:13]=[CH:12][CH:11]=[CH:16][CH:18]=1)=[O:1])[CH2:22][C:23]1[CH:28]=[CH:27][C:26]([O:29][CH3:30])=[CH:25][CH:24]=1参加物
4
実験手順
3.08 g of 2-benzyloxyphenylglyoxal hydrate (crude oil) are dissolved in 10 ml of dimethylsulfoxide, and 2.1 g of α-methyl-4-methoxyphenethylamine are added thereto. The mixture is stirred at room temperature for 45 minutes, whereby a solution of α-(α-methyl-4-methoxyphenethylimino)-2-benzyloxyacetophenone in dimethylsulfoxide is obtained.
出典と根拠
- ORDレコード
- ord-ba214585f48e496585b1c94fe26ae302
- 出典データセット
- uspto-grants-1984_12
- 特許番号
- US04490392
関連ノート
読み込み中…