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Dimethyl Sulfoxide → HCID 20434109、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Dimethyl Sulfoxide | HCID 679 | — |
| 反応物 | (+-)-p-Methoxyamphetamine | HCID 31721 | — |
| 反応物 | 2-Methoxyphenylglyoxal hydrate | HCID 20434110 | — |
| 生成物 | HCID 20434109 | HCID 20434109 | — |
反応手順
2.9 g of 2-methoxyphenylglyoxal hydrate (crude oil) are dissolved in 6 ml of dimethylsulfoxide, and 2 g of α-methyl-4-methoxyphenethylamine are added thereto. The mixture is treated in the same manner as described in Example 1-(2), whereby a solution of α-(α-methyl-4-methoxyphenethylimino)-2-methoxyacetophenone in dimethylsulfoxide is obtained.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04490392 |
| 出典データセット | uspto-grants-1984_12 |
| ORD ID | ord-0932d662c2e9447a9a8418898ede9ca9 |
| 出典メモ | uspto-grants-1984_12 |