Zirconium(IV) propoxide → HCID 86738105、化合物

HRID 1155180

反応式

HRID 1155180 の反応式
C[Si]([O:5][P:6]([CH2:13][CH2:14][CH2:15][CH2:16][C:17]([O:19][CH2:20][CH3:21])=[O:18])(=[O:12])[O:7][Si](C)(C)C)(C)C.[O-]CCC.[Zr+4:26].[O-]CCC.[O-]CCC.[O-]CCC>>[Zr:26].[C:17]([CH2:16][CH2:15][CH2:14][CH2:13][P:6](=[O:5])([O-:12])[O-:7])([O:19][CH2:20][CH3:21])=[O:18]

参加物

3

反応物 2

HCID 90139Zirconium(IV) propoxideHCID 20562960HCID 20562960、化合物

生成物 1

HCID 86738105HCID 86738105、化合物

実験手順

To a reaction flask under an inert atmosphere was added 3.13 g of bis-trimethylsilyl-4-carboethoxybutylphosphonate. To the flask was slowly added 1.44 g of zirconium propoxide. After the first few drops were added, a gelatinous product was formed. Agitation was continued during the remainder of the addition.

後処理

  1. additionAfter the first few drops were added
  2. customa gelatinous product was formed
  3. additionAgitation was continued during the remainder of the addition

出典と根拠

ORDレコード
ord-45ed4196492f405b81404d672065348d
出典データセット
uspto-grants-1981_11
特許番号
US04299943

関連ノート

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