関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Citric Acid | HCID 311 | — |
| 反応物 | Lithium Citrate | HCID 13520 | — |
| 反応物 | Sodium Chlorate | HCID 516902 | — |
| 反応物 | Sodium | HCID 5360545 | — |
| 溶媒 | Methanol | HCID 887 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | L-Ascorbic Acid | HCID 54670067 | — |
反応手順
7 grams of the sodium salt of 2,18-phosphomolybdic acid, 4 grams of sodium chlorate, 40 grams of citric acid, and 13.5 grams of trilithium citrate are dissolved in a mixture of 600 ml of methanol and 380 ml of water. A filter paper, for example Type 2668, made by the Schleicher & Schull Company, is impregnated with this solution, which has a pH-value of 3.6, and is dried for 1 hour at 60° C. Pieces measuring 6×6 mm are cut from the test paper prepared in this way, and sealed between a plastic handle and a thin nylon net, according to German Pat. No. 2 118 455. In urines with ascorbic acid in the important decision range of 0-40 mg of ascorbic acid/dl of urine, these test strips give very graduated reaction colors from bright greenish-blue to dark bluish-violet.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| 特許番号 | US04300905 |
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| 出典データセット | uspto-grants-1981_11 |
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| ORD ID | ord-d41d3a13ec7943aebedf8ccf30061f3d |
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| 出典メモ | uspto-grants-1981_11 |
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