Isobutyric Acid → Methylthiomethyl Isobutyrate

HRID 1155720ノート

反応式

HRID 1155720 の反応式
[C:1]([OH:6])(=[O:5])[CH:2]([CH3:4])[CH3:3].[CH3:7][S:8][CH2:9]Cl.C(N(CC)CC)C>>[C:1]([O:6][CH2:7][S:8][CH3:9])(=[O:5])[CH:2]([CH3:4])[CH3:3]

参加物

4

反応物 3

HCID 6590Isobutyric AcidHCID 8471TriethylamineHCID 16916Chloromethyl methyl sulfide

生成物 1

HCID 20481371Methylthiomethyl Isobutyrate

実験手順

This product was prepared according to the procedure described in Example 1, by reacting isobutyric acid with chloromethyl methyl sulfide in the presence of one equivalent of triethylamine; b.p. 64° C./12 mm Hg, nD20 1.4470.

後処理

  1. customThis product was prepared

出典と根拠

ORDレコード
ord-bd3e082e8ecd4a479789601898ea790b
出典データセット
uspto-grants-1982_06
特許番号
US04332829

反応ノート

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