Ethylformamide → N-alpha-Methoxyethyl-N-ethyl-formamide
反応式
[CH2:1]([NH:3][CH:4]=[O:5])[CH3:2].[CH3:6][O:7][CH:8](Cl)[CH3:9]>C(N(CC)CC)C>[CH3:6][O:7][CH:8]([N:3]([CH2:1][CH3:2])[CH:4]=[O:5])[CH3:9]参加物
4
実験手順
8.0 g of triethylamine and then a mixture of 42.5 g of triethylamine (0.5 mole in total) and 14.6 g (0.2 mole) of N-ethylformamide are added dropwise, at 0° C., to a mixture of 60 ml of light petroleum and 38 g (0.4 mole) of α-chloroethyl methyl ether.
出典と根拠
- ORDレコード
- ord-2642651a432646ebae59e346fac57c31
- 出典データセット
- uspto-grants-1982_06
- 特許番号
- US04334097
反応ノート
読み込み中…