Diethyl Ether → 2,3-Dimethyl-2-aminobutyronitrile hydrochloride

HRID 1156229ノート

反応式

HRID 1156229 の反応式
[C-:1]#[N:2].[K+].[CH3:4][CH:5]([CH3:9])[C:6](=O)[CH3:7].[Cl-:10].[NH4+:11].CCOCC>O>[ClH:10].[CH3:7][C:6]([NH2:11])([CH:5]([CH3:9])[CH3:4])[C:1]#[N:2]

参加物

6

反応物 4

HCID 3283Diethyl EtherHCID 9032Potassium CyanideHCID 112513-Methyl-2-butanoneHCID 25517Ammonium Chloride

生成物 1

HCID 129454442,3-Dimethyl-2-aminobutyronitrile hydrochloride

試薬・触媒・溶媒 1

HCID 962Water溶媒

実験手順

The reactant 2,3-dimethyl-2-aminobutyronitrile hydrochloride was prepared by the following reaction. A solution of 136 grams (g) (2.1 moles) of potassium cyanide in 220 milliliters (ml) of water was added dropwise at 10°-15° C. to a mixture of 172.2 g (2.0 moles) of 3-methyl-2-butanone, 110.2 g (2.1 moles) ammonium chloride, and 300 ml of ether. The mixture was allowed to reach room temperature at which it was stirred overnight.

後処理

  1. customto reach room temperature at which it

出典と根拠

ORDレコード
ord-51f7cd9ddd6e409594d72f31125435f6
出典データセット
uspto-grants-1982_06
特許番号
US04335053

反応ノート

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