4-Toluenesulfonyl chloride → 2-n-Butyl-5-tosyloxymethyl-4,5,6,7-tetrahydrobenzo[d]thiazole

HRID 1156968ノート

反応式

HRID 1156968 の反応式
[C:1]1([CH3:11])[CH:6]=[CH:5][C:4]([S:7](Cl)(=[O:9])=[O:8])=[CH:3][CH:2]=1.[CH2:12]([C:16]1[S:17][C:18]2[CH2:24][CH2:23][CH:22]([CH2:25][OH:26])[CH2:21][C:19]=2[N:20]=1)[CH2:13][CH2:14][CH3:15]>>[CH2:12]([C:16]1[S:17][C:18]2[CH2:24][CH2:23][CH:22]([CH2:25][O:26][S:7]([C:4]3[CH:5]=[CH:6][C:1]([CH3:11])=[CH:2][CH:3]=3)(=[O:9])=[O:8])[CH2:21][C:19]=2[N:20]=1)[CH2:13][CH2:14][CH3:15]

参加物

3

反応物 2

HCID 73974-Toluenesulfonyl chlorideHCID 129177552-n-Butyl-5-hydroxymethyl-4,5,6,7-tetrahydrobenzo[d]thiazole

生成物 1

HCID 543084972-n-Butyl-5-tosyloxymethyl-4,5,6,7-tetrahydrobenzo[d]thiazole

実験手順

The compound is prepared by action of p-toluenesulfonyl chloride on the above derivative (IV), according to the procedure described in Example 1. It is obtained as an undistillable oil which is used crude for the subsequent reactions.

後処理

  1. customIt is obtained as an undistillable oil which

出典と根拠

ORDレコード
ord-09fdc0708e1e4e2da9d38c4dba5d59b7
出典データセット
uspto-grants-1982_06
特許番号
US04337343

反応ノート

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