HCID 68695108、化合物 → HCID 68698459、化合物
反応式
[CH3:1][CH:2]([CH2:13][N+:14]([O-])=O)[CH2:3][C:4]([C:7]1[CH:8]=[N:9][CH:10]=[CH:11][CH:12]=1)([OH:6])[CH3:5]>CCO>[NH2:14][CH2:13][CH:2]([CH3:1])[CH2:3][C:4]([C:7]1[CH:8]=[N:9][CH:10]=[CH:11][CH:12]=1)([OH:6])[CH3:5]参加物
3
実験手順
Stir a mixture of 4-methyl-5-nitro-2-pyridin-3-yl-pentan-2-ol (860 mg, 3.84 mmol) and Pt—C(S) (200 mg) in EtOH (25 mL) at room temperature under hydrogen atmosphere (7 atm) for 24 h. Filter through a pad of Celite® and evaporate to obtain 630 mg (84%) of the title compound.
後処理
- filtrationFilter through a pad of Celite®
- customevaporate
出典と根拠
- ORDレコード
- ord-5819c264c2664d79a296e1d500c00303
- 出典データセット
- uspto-grants-2010_10
- 特許番号
- US07807691B2
反応ノート
読み込み中…