化工社化工社 化学情報印刷レポート · 研究参考用
Acetonitrile → Carbamic chloride, N-ethyl-N-(phenylmethyl)-
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Acetonitrile | HCID 6342 | — |
| 反応物 | N-Ethylbenzylamine | HCID 84352 | — |
| 反応物 | N-benzyl-N-methylcarbamoyl chloride | HCID 10464985 | — |
| 反応物 | Acetonitrile--water (1/1) | HCID 18373917 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | Carbamic chloride, N-ethyl-N-(phenylmethyl)- | HCID 10679448 | — |
反応手順
The title compound is prepared analogously as described for benzyl-methyl-carbamoyl chloride from benzyl ethylamine. MS (LC-MS): [M+H]+=198.1. tR (HPLC, Waters Symmetry C18 column, 20-95% CH3CN/H2O/3.5 min, 95% CH3CN/H2O, 2 min, CH3CN and H2O containing 0.1% TFA, flow: 0.6 mL/min): 4.12 min.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07807709B2 |
| 出典データセット | uspto-grants-2010_10 |
| ORD ID | ord-47c738335f46429ebba8e9c517f0ea16 |
| 出典メモ | uspto-grants-2010_10 |