Hydrochloric Acid → 6-(3-Chlorophenoxy)-o-cresol

HRID 1164009ノート

反応式

HRID 1164009 の反応式
[CH3:1][C:2]1[CH:8]=[CH:7][CH:6]=[C:5]([O:9][C:10]2[CH:15]=[CH:14][CH:13]=[C:12]([Cl:16])[CH:11]=2)[C:3]=1N.Cl.[OH2:18]>>[Cl:16][C:12]1[CH:11]=[C:10]([CH:15]=[CH:14][CH:13]=1)[O:9][C:5]1[CH:6]=[CH:7][CH:8]=[C:2]([CH3:1])[C:3]=1[OH:18]

参加物

4

反応物 3

HCID 313Hydrochloric AcidHCID 962WaterHCID 205134252-(3-Chlorophenoxy)-6-methylaniline

生成物 1

HCID 205135046-(3-Chlorophenoxy)-o-cresol

実験手順

A mixture of 2-methyl-6-(3-chlorophenoxy)aniline (40 g) and conc. hydrochloric acid (36 ml) in water (125 ml) was treated in a similar manner to that of Example 6-(1) to give oily 6-(3-chlorophenoxy)-o-cresol (13.9 g)

後処理

  1. additionwas treated in a similar manner to that of Example 6-(1)

出典と根拠

ORDレコード
ord-2b710e4c10684ffbacf46a40a329ef03
出典データセット
uspto-grants-1983_01
特許番号
US04367238

反応ノート

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