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Dimethyl Sulfate → Phenyl 2-methoxy-3-methylphenyl ether
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Dimethyl Sulfate | HCID 6497 | — |
| 反応物 | Potassium Hydroxide | HCID 14797 | — |
| 反応物 | 6-Phenoxy-o-cresol | HCID 22734681 | — |
| 溶媒 | Ethanol | HCID 702 | — |
| 生成物 | Phenyl 2-methoxy-3-methylphenyl ether | HCID 20082997 | 74.8% |
反応手順
A mixture of 6-phenoxy-o-cresol (7.5 g) and dimethyl sulfate (14 g) and aqueous solution (30 ml) of potassium hydroxide (10.5 g) were treated in a similar manner to that of Example 14-(2). The resultant residue was pulverized with ethanol to give phenyl 2-methoxy-3-methylphenyl ether (6 g). mp 52°-53° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04367238 |
| 出典データセット | uspto-grants-1983_01 |
| ORD ID | ord-1184ecfe4267478496a28147cca519d9 |
| 出典メモ | uspto-grants-1983_01 |