Potassium Iodide → HCID 70529163、化合物
反応式
[CH3:1][N:2]1[C@@H:11]2[CH2:12][C:13]3[C:18]([C:9]4=[C:10]2[C:5](=[CH:6][C:7]([O:25][CH3:26])=[C:8]4[O:23][CH3:24])[CH2:4][CH2:3]1)=[CH:17][C:16]([O:19][CH3:20])=[C:15]([O:21][CH3:22])[CH:14]=3.[I-:27].[K+]>Cl>[CH3:1][N:2]1[C@H:11]2[CH2:12][C:13]3[C:18](=[CH:17][C:16]([O:19][CH3:20])=[C:15]([O:21][CH3:22])[CH:14]=3)[C:9]3[C:10]2=[C:5]([CH:6]=[C:7]([O:25][CH3:26])[C:8]=3[O:23][CH3:24])[CH2:4][CH2:3]1.[IH:27]参加物
4
実験手順
For making l-glaucine hydroiodide, a quantity of l-glaucine was dissolved in 2 n hydrochloric acid and the solution reacted with saturated potassium iodide solution. The resulting crystalline precipitate was recrystallized from a mixture of methyl alcohol and ether. This gave a crystalline, yellowish glaucine hydroiodide with a melting point of 238° C.