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2,3-Dihydrobenzo(b)furan-5-carboxylic acid → HCID 12985421、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2,3-Dihydrobenzo(b)furan-5-carboxylic acid | HCID 676583 | — |
| 反応物 | 6,11-dihydro-5H-pyrido[2,3-b][1,5]benzodiazepine | HCID 11030760 | — |
| 溶媒 | Diethyl Ether | HCID 3283 | — |
| 生成物 | HCID 12985421 | HCID 12985421 | — |
反応手順
Prepared from 2,3-dihydro-benzofuran-5-carboxylic acid (0.328 g, 2 mmol) and 6,11-dihydro-5H-pyrido[2,3-b][1,5]benzodiazepine (0.398 g, 2 mmol) in a manner essentially identical to that of Example 1. The title compound was obtained as an off-white solid, m.p. 188° C., upon recrystallization from diethyl ether.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06620807B1 |
| 出典データセット | uspto-grants-2003_09 |
| ORD ID | ord-7e0f7c5ba55f435f9ef9813b3924f07a |
| 出典メモ | uspto-grants-2003_09 |