1-(4-Benzyloxy-phenyl)-2-pyridin-4-yl-ethanone → 2-Pyridin-4-yl-1-(4-triisopropylsilanyloxymethyl-phenyl)-ethanone
反応式
C(O[C:9]1[CH:14]=[CH:13][C:12]([C:15](=[O:23])[CH2:16][C:17]2[CH:22]=[CH:21][N:20]=[CH:19][CH:18]=2)=[CH:11][CH:10]=1)C1C=CC=CC=1.CON(C)C(=O)C1C=CC([CH2:34][O:35][Si:36]([CH:43]([CH3:45])[CH3:44])([CH:40]([CH3:42])[CH3:41])[CH:37]([CH3:39])[CH3:38])=CC=1>>[N:20]1[CH:19]=[CH:18][C:17]([CH2:16][C:15]([C:12]2[CH:11]=[CH:10][C:9]([CH2:34][O:35][Si:36]([CH:37]([CH3:39])[CH3:38])([CH:43]([CH3:45])[CH3:44])[CH:40]([CH3:42])[CH3:41])=[CH:14][CH:13]=2)=[O:23])=[CH:22][CH:21]=1参加物
3
実験手順
Following the procedure for the preparation of 1-(4-Benzyloxy-phenyl)-2-pyridin-4-yl-ethanone but substituting N-Methoxy-N-methyl-4-triisopropylsilanyloxymethyl-benzamide provided the title compound. MS: (M+H m/z=384.1).
出典と根拠
- ORDレコード
- ord-1bb38e02ce1943c985a54766daf2a00d
- 出典データセット
- uspto-grants-2010_11