Carbon Dioxide → HCID 178527662、化合物

HRID 1172027ノート

反応式

HRID 1172027 の反応式
[CH2:1]([S:6]([OH:9])(=[O:8])=[O:7])[S:2]([OH:5])(=[O:4])=[O:3].C(=O)([O-])[O-].[Ag+2:14].C(=O)=O>O>[CH2:1]([S:6]([O-:9])(=[O:8])=[O:7])[S:2]([O-:5])(=[O:4])=[O:3].[Ag+2:14]

参加物

5

反応物 3

HCID 280Carbon DioxideHCID 10427Methanedisulfonic acidHCID 178418647HCID 178418647、化合物2 回

生成物 1

HCID 178527662HCID 178527662、化合物

試薬・触媒・溶媒 1

HCID 962Water溶媒2 回

実験手順

A 50% solution of methanedisulfonic acid in water (2.5 grams) was diluted in 25 mL of water into which, while stirring, silver carbonate (3.91 grams) was added slowly. The silver carbonate dissolved with effervescence of carbon dioxide. After the reaction was complete remaining insoluble material was removed by filtration and the filtrate was stripped of water and dried under high vacuum at 45° C. to give 4.9 grams of white crystals.

後処理

  1. customwas removed by filtration
  2. customdried under high vacuum at 45° C.

出典と根拠

ORDレコード
ord-7bd1a6dd4a404260a7cdcc8cbba5a5f7
出典データセット
uspto-grants-2010_11
特許番号
US07833693B2

反応ノート

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