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HRID 1174965作成日：2026年10月27日

3-Phenoxybenzoic acid → n-{2-[(2-Dimethylamino-ethyl)-methyl-amino]-benzothiazol-6-yl}-3-phenoxy-benzamide

https://huagongshe.com/reaction/1174965

反応式

関与物質

役割名称HCID仕込み量
反応物3-Phenoxybenzoic acidHCID 19539—
反応物N2-(2-Dimethylamino-ethyl)-N2-methyl-benzothiazole-2,6-diamineHCID 55226563—
生成物n-{2-[(2-Dimethylamino-ethyl)-methyl-amino]-benzothiazol-6-yl}-3-phenoxy-benzamideHCID 57771758—

反応手順

The title compound is prepared by following General Method A, using 3-phenoxy-benzoic acid (0.22 g, 1.04 mmol), and N*2*-(2-dimethylamino-ethyl)-N*2*-methyl-benzothiazole-2,6-diamine (0.20 g, 0.80 mmol) to afford an off-white solid (0.19 g, 53%). LC/MS: Retention time=4.45 nm in; (m/z): calcd for C25H2(N4O2S (M+H)+: 447.6; found: 447.3.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US07838543B2
出典データセットuspto-grants-2010_11
ORD IDord-8ec71a69e9324abe86eeb9dbc601afe3
出典メモuspto-grants-2010_11