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4-(Thiophen-2-yl)benzoic acid → HCID 57771755、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 4-(Thiophen-2-yl)benzoic acid | HCID 736498 | — |
| 反応物 | N2-(2-Dimethylamino-ethyl)-N2-methyl-benzothiazole-2,6-diamine | HCID 55226563 | — |
| 生成物 | HCID 57771755 | HCID 57771755 | — |
反応手順
The title compound is prepared by following General Method A, using 4-thiophen-2-yl-benzoic acid (0.098 g, 0.48 mmol), and N*2*-(2-dimethylamino-ethyl)-N*2*-methyl-benzothiazole-2,6-diamine (0.10 g, 0.40 mmol) to afford the title compound as a white solid. LC/MS: Retention time=4.37 min; (m/z): calcd for C23H24N4OS2 (M+H)+: 437.6; found: 437.3.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07838543B2 |
| 出典データセット | uspto-grants-2010_11 |
| ORD ID | ord-a38f28e84e2a4225ba11329854baad27 |
| 出典メモ | uspto-grants-2010_11 |