5-ethoxy-benzothiazol-2-ylamine → HCID 86611016、化合物

反応式

[CH3:1][C:2]1([CH3:15])[O:11][C:10]2[C:5](=[CH:6][C:7]([C:12]#[N:13])=[CH:8][CH:9]=2)[CH:4]2[O:14][CH:3]12.[CH2:16]([O:18][C:19]1[CH:20]=[CH:21][C:22]2[S:26][C:25]([NH2:27])=[N:24][C:23]=2[CH:28]=1)[CH3:17]>>[CH2:16]([O:18][C:19]1[CH:20]=[CH:21][C:22]2[S:26][C:25]([NH:27][CH:4]3[C:5]4[C:10](=[CH:9][CH:8]=[C:7]([C:12]#[N:13])[CH:6]=4)[O:11][C:2]([CH3:15])([CH3:1])[CH:3]3[OH:14])=[N:24][C:23]=2[CH:28]=1)[CH3:17]

参加物

反応物 2

HCID 8212115-ethoxy-benzothiazol-2-ylamine

HCID 108673602,2-Dimethyl-3,4-epoxy-6-cyanochroman

生成物 1

HCID 86611016HCID 86611016、化合物

実験手順

Following the procedure in Example 1, using (±)-2,2-dimethyl-1a,7b-dihydro-2H-1,3-dioxa-cyclopropa[a]naphthalene-6-carbonitrile and 5-ethoxy-benzothiazol-2-ylamine as starting material, the title compound was prepared as a white solid.

出典と根拠

ORDレコード: ord-b8622517cdf94ba381e3516fee4b9a30
出典データセット: uspto-grants-2010_11
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US07838553B2

反応ノート

読み込み中…