Methanesulfonyl chloride → 2-{3-[(Methylsulfonyl)amino]phenyl}ethyl methanesulfonate

HRID 1179627

反応式

HRID 1179627 の反応式
[NH2:1][C:2]1[CH:3]=[C:4]([CH:8]=[CH:9][CH:10]=1)[CH2:5][CH2:6][OH:7].[CH3:11][S:12](Cl)(=[O:14])=[O:13]>>[CH3:11][S:12]([O:7][CH2:6][CH2:5][C:4]1[CH:8]=[CH:9][CH:10]=[C:2]([NH:1][S:12]([CH3:11])(=[O:14])=[O:13])[CH:3]=1)(=[O:14])=[O:13]

参加物

3

反応物 2

HCID 31297Methanesulfonyl chlorideHCID 149389872-(3-Aminophenyl)ethan-1-ol

生成物 1

HCID 574443592-{3-[(Methylsulfonyl)amino]phenyl}ethyl methanesulfonate

実験手順

The title compound was prepared from 3-aminophenethyl alcohol (U.S. Pat. No. 2,641,602) and methanesulfonyl chloride (2 eq.) according to the procedure contained within description 4. The product was used immediately without further purification or characterisation.

後処理

  1. customThe product was used immediately without further purification or characterisation

出典と根拠

ORDレコード
ord-445e0645ee6447be81cd475dfdd82f0e
出典データセット
uspto-grants-2007_10
特許番号
US07279481B2

関連ノート

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