3-(2,6-dichloro-benzyl)-6-chloro-7-hydroxy-4-methyl-2H-chromen-2-one → Methyl-phenyl-carbamic Acid 3-(2,6-dichloro-benzyl)-6-chloro-4-methyl-2-oxo-2H-chromen-7-yl Ester
反応式
[Cl:1][C:2]1[CH:22]=[CH:21][CH:20]=[C:19]([Cl:23])[C:3]=1[CH2:4][C:5]1[C:6](=[O:18])[O:7][C:8]2[C:13]([C:14]=1[CH3:15])=[CH:12][C:11]([Cl:16])=[C:10]([OH:17])[CH:9]=2.[I-].[CH3:25][N:26]([C:35]1[CH:40]=[CH:39][CH:38]=[CH:37][CH:36]=1)[C:27](N1C=C[N+](C)=C1)=[O:28]>>[Cl:1][C:2]1[CH:22]=[CH:21][CH:20]=[C:19]([Cl:23])[C:3]=1[CH2:4][C:5]1[C:6](=[O:18])[O:7][C:8]2[C:13]([C:14]=1[CH3:15])=[CH:12][C:11]([Cl:16])=[C:10]([O:17][C:27](=[O:28])[N:26]([CH3:25])[C:35]1[CH:40]=[CH:39][CH:38]=[CH:37][CH:36]=1)[CH:9]=2参加物
3
実験手順
The title compound was prepared from 3-(2,6-dichloro-benzyl)-6-chloro-7-hydroxy-4-methyl-2H-chromen-2-one and 3-(methyl-phenyl-carbamoyl)-1-methyl-3H-imidazol-1-ium iodide. HPLC-MS m/z=502 (M+1), Rt: 5.68 min.
出典と根拠
- ORDレコード
- ord-a9ade9fa34244a1b8c60a3221a91e484
- 出典データセット
- uspto-grants-2007_10