2-Methyl-5-hydroxypyridine → Methyl-phenyl-carbamic Acid 6-methyl-pyridin-3-yl Ester

HRID 1179797

反応式

HRID 1179797 の反応式
[OH:1][C:2]1[CH:3]=[N:4][C:5]([CH3:8])=[CH:6][CH:7]=1.[CH3:9][N:10]([C:14]1[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1)[C:11](Cl)=[O:12]>>[CH3:8][C:5]1[N:4]=[CH:3][C:2]([O:1][C:11](=[O:12])[N:10]([CH3:9])[C:14]2[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=2)=[CH:7][CH:6]=1

参加物

3

反応物 2

HCID 142752-Methyl-5-hydroxypyridineHCID 77969Carbamic chloride, N-methyl-N-phenyl-

生成物 1

HCID 69518367Methyl-phenyl-carbamic Acid 6-methyl-pyridin-3-yl Ester

実験手順

The title product was prepared from 3-hydroxy-6-methyl-pyridine and N-methyl-N-phenylcarbamoyl chloride. The crude product was subjected to preparative HPLC. (79%, colourless oil). HPLC-MS: m/z=243.1 (M+1); Rt: 2.24 min.

出典と根拠

ORDレコード
ord-6b1c434ab0af4d479c1d78728ac0c500
出典データセット
uspto-grants-2007_10
特許番号
US07279470B2

関連ノート

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